Split/Splitless Capillary
•Range to 400 °C in 1 °C
increments
•Back-pressure design permits
independent adjustment of splitflow rate without affecting
column flow, 0–30 psi head pres-sure gauge, and regulator•Septum purge built in at
3 mL/min
•Accepts columns up to 1.2-mm od•Accepts 1/4-in. glass column for
on-column injection
•Multimode design includes split
and splitless injection
•Air fan built into mainframe to
assist in cool-down of inlet•Splitless purge time variable in
0.01-min elements
Packed with Septum Purge
•Range to 400 °C in 1 °C
increments
•Flow control/forward-pressure
design, 0–100 psi head pressuregauge
•Septum purge built in at
1.5 mL/min
•On-column injection available
with configuration A, 1/4-in. odglass columns
•Individual liners for use with 1/8-and 1/4-in. metal columns as wellas for Series 530-µm columns•Liners available for use with
replaceable glass inserts
•Air fan built into mainframe to
assist cool-down of inlet
2
Detectors
Thermal Conductivity Detector
•Range to 400 °C
•Single-filament (single-column)
design has fluidic switching ofreference and analytical carrierflows; a passivated tungsten-rhenium filament is used in a 3.5-µL cell operating at a con-stant temperature difference rel-ative to the detector blocktemperature
•Minimum detectable: <400 pg/mL
carrier—equivalent to <1 ppm ofneon in 1 mL of air (may beadversely affected by acousticnoise in the laboratory environment)
•Linear dynamic range: <±5% over
105range
•Digital gain setting time–pro-grammable through the keyboardConditions: detector 100 °C, 45 mL/min switching and 30 mL/min analytical flow ofhelium, propane sample
3
Flame Ionization Detector
•Range to 450 °C
•Grounded jet and current limited
design for operator safety•Push-button flame ignition•Fused silica columns insert
within 2 mm of the jet tip•Sensitivity:
–>18 mCoul/g carbon:
nitrogen carrier, 0.018-in. id jet–>15 mCoul/g carbon:
helium carrier, 0.018-in. id jet –>22 mCoul/g carbon:
nitrogen carrier, 0.011-in. idcapillary jet
–>18 mCoul/g carbon:
helium carrier, 0.011-in. id capillary jet
•Minimum detectable: <5 pg
carbon/sec, nitrogen carrier atS/N=2
•Linear dynamic range: <±10%
over a 107range with 0.018-in. idjetConditions: column flow 50 mL/min,45 mL/min H2, 650 mL/min air,propane sample
Electron Capture Detector
•Range to 400 °C
•A coaxial design with a 15 mCi
source (555 MBq) of Ni–63plated on the interior of thelower block
•Constant current mode of opera-tion features switch selection ofpulse parameters for using eithernitrogen, hydrogen, helium, orargon/methane carrier gas•Minimum detectable level:
<0.04 pg/sec lindane
•Dynamic range: >104for lindaneConditions: detector 250 °C, 60 mL/min nitrogen carrier
Column Oven
•Usable volume:
–11 in. × 12 in. × 6.5 in. (h × w × d)
–279 mm × 305 mm × 165 mm (h × w × d)•Column span: 228.5 mm, 9 in. (coil size)
•Automatic cooling under processor control•
Operating range:
4 °C above ambient to 450 °C:80 to 450 °C with cryogenic cooling
•
Setpoint entry:
–1 °C for temperatures–0.1 °C for program rates•
Programming:
–Rates 0.1 to 70 °C* per min–650 min maximum run time–Three ramps withinitial/final holds
Technical Performance
•Accuracy (true temperature rela-tive to setpoint)
Specification: +1% (°K) from 4 °Cabove ambient to 450 °C•Stability (effect of ambient
change on actual temperature)Specification: <0.01 °C for 1 °C ambient change
•Calibration (setting true temper-ature at a setpoint)
Oven can be recalibrated to ±0.01 °C with appropriate instrumentation
+0.075+0.21+0.050100 ˚C Oven+0.037-0.40300 ˚C Oven-0.460.00-0.58Oven Heating ProfilesTemp (˚C)Temp (˚C)300118 Vac240 Vac108 Vac300One Series 530-injection port, and one detectorµ column, oneat 300 200108 Vac Curve: One emptyfor 1 hour prior to cooldown)˚C (oven held at 300 ˚C20010-ft ss column; injectionport and detector unheated100118/220 Vac: One Series530-10050port, and one detector at 300 µ column; one injection˚C0246810125002468Time (min)Time (min)•Gradients (temperature varia-tions within a column)
Specification: less than 2 °Cwithin a 9-in. coil anywherewithin the operating range*Achievable rates depend on zonetemperature, voltage, and columns.
Agilent shall not be liable for errors contained herein orfor incidental or consequential damages in connectionwith the furnishing, performance, or use of this material.
Information, descriptions, and specifications in thispublication are subject to change without notice.Copyright© 2000
Agilent Technologies, Inc.Printed in the USA 6/2000(23) 5968-4475EN
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